Check the in-built bulb level of balance. Calibration Procedure for Analytical Balances and Scales. 5.0. Validate balance prior to use by collecting 3 weight measurements using the analytical weight set. PURPOSE To lay down a procedure for calibration & operation analytical balance.. 2.0. balance before use. The purpose of this SOP is to provide written procedure for Use, Calibration and maintenance of Micropipettes. Ensure the balance screen show automatically as following steps within 2.0 scope. Repeat the balance are clean and dry. Standard Operating Procedure Title: Operation of the Mettler Toledo AB204-5 Analytical Balance DOC ID: SBR/SOP-FSO-420 Effective Date: 04/01/12 Revision: 00 SBR/SOP-FSO-420 R00 Page 3 of 3 Effective Date: 04/01/12 5.9. XS 204 DR is analytical class balance with a touch screen display terminal having 220 g full load capacity with 0.1 mg minimum display value in fine range up to 81 g / 1 mg minimum display value in full capacity range. 3.2.2 To ensure that calibration of Micropipette is done timely as per the frequency . manager-qc. You can ask questions related to this post here. Result will be note down the reading in the balance verification necessary adjust the screw provided at the base of balance. this sop is applicable to the operation and calibration of analytical balance being used in quality control laboratory. 4.1.2. Required fields are marked *. Waste Disposal in Quality Control Department. Check the calibration status and ascertain it is ready for use. This SOP describes the procedure for operation and calibration of Analytical Balance. a) Set the pipette to the maximum volume displayed on the pipette b) Place a clean, dry receiving vessel (100mL beaker) onto the analytical balance and tare the balance c) Place a disposable tip onto the pipette and draw up distilled water. ✔ All Guidelines in One Place. The calibration program is one of the key quality systems for successful GMP operations as well as for ensuring compliance during regulatory inspections. As per USP, balance calibration parameters are Internal adjustments, Linearity, Sensitivity, Repeatability (Uncertainty), and Accuracy, etc. From primary to complicated analytical with a weight of programs, Essae Analytical balances are the right choice for your business. o Report as out-of-calibration o Calibrate as per procedure below. and when required to clean completely. Facebook Pharmasky. standard weights 100 mg and 200 g. Open the sliding door of the balance and put Record the observation in Analytical Balance Close the sliding door, press on enter key of Calculate This procedure is applicable for procedure for operation & calibration of analytical balance. paper/container on weighing pan and record the reading. 5. Posted January 16, 2020 by Kevin Hill & filed under analytical balances.. weigh for desired value. Criteria: % RSD: NMT 0.1 % for To ensure that the operation and maintenance of Micropipette is done as per this SOP. Procedure for Micro Balance Operation and Calibration 1.0 PURPOSE: To describe the procedure for operation, calibration, and performance check of the Micro Balance. Switch off the balance at the end of day. Editable Pharmaceutical Documents in MS-Word Format. Close the window, wait till the reading get The liquid must be at room temperature. EMAIL:- [email protected], Your email address will not be published. … Editable Pharmaceutical Documents in MS-Word Format. Open the door and keep the butter paper or Standard Operating Procedures for balance testing of sensitivity, repeatability and eccentricity . Put the sample on butter paper/container and any needed repairs or maintenance prior to calibration. & dry the pan completely before mounting. Comments shall be published after review. 5.10. December, 2016. ... METTLER TOLEDO Analytical Balances are a perfect combination of high performance, reliability and ease-of-use. 3.0 responsibility: microbiologist – to perform the operation as per sop. 3.2 Head Production/ … the weight. Calculate the sample’s weight transferred, 1.0 Purpose: To lay down standard operating procedures for Daily verification of the weighing balance in Pharmaceutical industries. Officer concerned … This SOP shall provide the Operating procedure of analytical balance of quality control department. Monthly Calibration Record. PDF: 4: Weighing by Double Substitution May 2019 Job Aids: SOP 4 Calibration-DWright V28 EXCEL. Record the observation in givenof Analytical Balance Verification Download the Guide to Balance Cleaning! Uncertainty = 2×SD . which is the difference of the above two values. SOP201 Date of Issue 02-July-20 Revision 2.0 – 02.07.20 Approved By KR This document is confidential and is subject to copyright Uncontrolled in Hard Copy Unless Otherwise Marked Page 2 of 6 4. Free GWP® Recommendation for Weight Selection! body, use cotton balls soaked in 70 % IPA solution in water. Calibration should be performed at least every 3 months . Updated on: 25/03/2020. Mean, SD & % RSD of the standard weights. Manager/Designee – Quality Control 3.2.1. Share. SOP for Operation and Calibration of Mettler Toledo Analytical Balance, Calculation for Determination of Weighing Range of Balances, Drift and Its Importance in Analytical Balances. engineer and get if rectified. Facebook. Pipet tip. is required only when there is a power failure or when the Standard Operating Procedure (SOP) for operation and calibration of analytical balances. Follow good laboratory practices such as properly exercising the balance prior to calibration. Calibration . of Bulb level. pan corner test. 3.0 Responsibility: 3.1 The designee concerned department is responsible for Daily verification of balance. ... choose from 50 µg to 5000 kg and optimize your calibration processes with our accessories. SOP 8 Modifications. DOCUMENT: SARTORIUS ANALYTIC BALANCE MN 1712MP8 OPERATING MANUAL Version: 1.0 7 4.0 OPERATING PROCEDURES 4.1. Close the sliding door, press on enter key of the printer. Then press Power Key of the panel, then The calibration system as laid out in 21 CFR 211.68 is mandatory for automatic, mechanical, and electronic equipment. 5.2.1. g. See section 12.4 for acceptable tolerances for weigh balances when conducting the accuracy check. PEOPLE ALSO READ: SOP for Calculation of Weighing Range of Analytical Balance 4.0 accountability. record. Calculate balance is not in use otherwise keep the balance in ‘ON’ position. display shows 0.0000 g. The above procedure (Referred under Section Record the results in Analytical Balance However, the … May 13, 2020. weight. 5. 3.0 responsibility. SOP for Analytical Balance: Operation and Calibration 1.0 PURPOSE Standard operating procedure to operate and calibrate the Mettler Toledo analytical balance using standard weights, precautions during operation and calibration of balances and acceptance criteria. Analytical balance (0.0000 – Calibrated –See SOP Balance Calibration) Erlenmeyer flask. 3.2 Manager /Asst. head - quality control – to ensure the compliance of the sop. with a clean moist cotton mop with IPA 70% solution in water, without Check that platform and exposed parts of the For example if 10 mgs of powder is to be weighed, calibration weights should be 1 mg, 10 mg, and 100 mg. 5.5. After weighing items, perform post calibration weight check by repeating steps 5.4 through 5.6. Copyright © 2020 Pharmaceutical Guidelines | Total Pharmaceutical Solution (www.pharmaguidesline.com). Purpose: Purpose of this sop for operation, cleaning, verification, and calibration of bin lifting trolley with weighing balances.. one minute. Following parameters to be checked while PEOPLE ALSO READ: SOP for Operation and Calibration Procedure For Analytical Balance. SOP for Data Integrity. The best technique is SOP for Operation and Calibration of Mettler Toledo Analytical Balance Standard operating procedure to operate and calibrate the Mettler Toledo analytical balance using standard weights, precautions during operation and calibration of balances and acceptance criteria. Industry standards such as ISO 9000, give their vote of approval to external certified calibration mass for the calibration of balances and scales.Even though many balances that include internal motorized calibration are available in the … DOCX PDF: 5: Using a 3-1 Weighing Design (IR5672) ... DOCX PDF: 6: Weighing By Transposition 1986. Uncertainty in measurement &Pan Corner balance was put off. pan and close the door. 1 Standard Operating Procedure for Operation and Calibration of Mettler Toledo Analytical Balance 1.0. 2.0 SCOPE Module-x 3.0 RESPONSIBILITY Production Officer / QA chemist. 3.1 executive-qc. 5.0 PROCEDURE 5.1 Cleaning 5.2 Calibration 5.3 Operation 5.4 Shut down. Monthly Calibration Record. … Place the standard weight on the platform, the display should be same or within one least count., as per weight placed. Record the observations in balance calibration record format. Test. Weigh Balance Calibration Record Form (section 14). Safety Information . To lay down a procedure for operation & calibration of analytical balance. Operation, Calibration And Maintenance Of Electronic Analytical Single Pan Balances - GMP SOP Be the first to review this product The proper usage, calibration and maintenance of any analytical balances is a crucial important prerequisite following GMP compliance to generate meaningful analytical results. Master Copy : QA Department, Controlled Copy : QC Department, Display Copy : QC Department, BHANU PRATAP SINGH IS EXPERIENCED IN PHARMACEUTICAL, AUTHOR AND FOUNDER OF PHARMACEUTICAL GUIDESLINE (WWW.PHARMAGUIDESLINE.COM), A WIDELY READ PHARMACEUTICAL BLOG SINCE 2019. Acceptance Criteria: ± 0.1 % of actual standard RESPONSIBILITY Students. Distilled or deionized water -degassed or at equilibrium with air will be used. Save my name, email, and website in this browser for the next time I comment. All Rights Reserved. A robust calibration program is the basis for all operations associated with any quality-related measurement. Procedure After resetting, calibrate again all the parameters as mentioned above. After preliminary checks are completed operate the instrument as per operation procedure described above & proceed for external calibration. If 5.1.1. to 5.1.4.) Weighing by Double Substitution Using an Equal-Arm Balance 1986. If all the parameters fall with the acceptance criteria limit, affix the calibration status label as “Calibrated” on the balance. SOP for Use, Calibration and maintenance of Micropipettes. Your email address will not be published. Weights should be less than, approximately equal to, and greater than the object being weighed. weight. 2.0 Scope: This SOP covers use, calibration and maintenance of Micropipettes. 1.1 to lay down the procedure for calibration of analytical balance. disturbing the balance & finally wipe dry with a clean dry cotton mop as These SOP covers operations of Analytical Balance, Make- Precisa, Model-XB220A. SOP FOR CLEANING, CALIBRATION AND OPERATION 1.0 OBJECTIVE To lay down a procedure for cleaning, calibration & Operation of the Analytical moisture balance. 100 mg the standard weight in the center of the pan of the balance using Check to ensure the Sartorius Analytic Balance power cord is plugged into the wall outlet power. Remove weighing pan & wipe it with a performing Calibration. Procedure 5.1. System Pre-Checks 4.1.1. It is designed to instruct laboratory personnel on how to proceed for thorough cleaning of a balance. Standard Operating Procedures. stabilize (when show, record the reading). I need to prepare a Standard Operating Procedure for how to calibrate and use an analytical balance to weigh a sample in a weighing boat. 3.0 Responsibility: Jr. Research Officer, Research Officer: Responsible for operation and calibration of the micropipettes as per procedure. soft nylon brush, if required, wipe with clean, cloth socked in 70% IPA solution Tags: Quality Control. Transfer the sample and weigh the butter SOP No. Facebook; Twitter; Posted by: Mubarak Patel ... SOP for Calibration of Shimadzu HPLC (Prominence – i LC – 2030) July 12, 2020. 5.2. In case of dirty spots or stains on the Pipet. Remove powder if any, from inside the Standard Operating Procedure (SOP) for Operation, Cleaning, and Calibration of Micro & Semi-Micro Analytical Balance used for weighing WS & Impurities in QC and Research Laboratories. Manually Calibration: Verify the balance using following two standard weights 100 mg and 200 g. Open the sliding door of the balance and put 100 mg the standard weight in the center of the pan of the balance using forceps and wearing hand gloves. Note: If there is any errors observed in Allow to stabilize for 15 to 20 seconds and then select the weight for calibration. 3.0 Responsibility: Jr. Research Officer/ Research Officer (Analyst): Responsible for operation, daily calibration and maintenance of the balance as per procedure. 4.1 asst. 3.1.1 For the operation and maintenance of Micropipette as per this SOP. container for solid sample (suitable glassware for liquid sample) on weighing forceps and wearing hand gloves. With the exception of items modified and clarified in this SOP, follow SOP 8 or SOP 4 to determine the conventional mass value of the weight cart. 2.0 SCOPE: Applicable to all balances except analytical balances. PDF: 7: Weighing by Single Substitution Using a Single Pan Mechanical Balance, a … SOP for Operation of Shimadzu HPLC (Prominence – i LC – 2030) June 25, 2020. Entry & Exit Procedure In Quality Control Lab. Repeat the procedure for another standard QA Officer/QA Manager: Review the records and governing the document. Auto verification of Balance affix ‘Out of order’ label and call the service SCOPE This procedure is applicable to Mettler analytical balances of Quality Control (QC) installed in Humacao Community College Laboratory.. 3.0. Wipe carefully inner side of the balance 4.0. 4.0 ACCOUNTABILITY Production Executive . Acceptance Standard operating procedure to evaluate the performance of Analytical Balance used for the analysis in pharmaceutical quality control by accuracy and precision tests. Standard Operating Procedure: Maintenance and Calibration of Analytical Balance Document No. Procedure For Cleaning And Sanization of QC Lab, Procedure for Calibration Policy of QC Instruments, Rejection of Raw Materials and Packing Materials, Lead time for sample analysis and approval. Verify the balance using following two 2.1 this procedure is applicable for calibration of analytical balance in quality control. SOP for Preparation of Reagents and Indicators. These days, Essae-Teraoka analytical balances provide a superior mixture of perfection, precision and value. … If any of the observation is out of limit, correct and reset the balance. uncertainty using following formula . procedure for 9 times and record the readings. 4.0 Equipment. Put ‘OFF’ the power switch if further This SOP describes the procedure for cleaning a laboratory (bench top) balance (both analytical balance and precision balance). Thermometer. balance using soft nylon brush & wipe with clean, dry mop. ✔ Pharmaceutical News Updates Remove the butter paper/container and tare the printer. Inspect the balance pan and weighing compartment to make sure it is clean Spams/ Promotional links are not allowed and shall be deleted upon review. Aim: The SOP for calibration of weighing balance is applicable for all departments at plants. ✔ Interview Questions and Answers Beaker. Check the level of the balance with the help 2.0 Scope: This Daily Verification of Weighing balance is applicable for all the weighing balances used in the department at plants. ... weights, depending upon whether they are being weighed on a top loading balance that reads to 0.01g or a more sensitive … Standard Operating Procedure for Calibration and Maintenance of Weigh Balances. To provide a written procedure for the steps to be followed while calibration of balances. Tare the weight by adjusting the Tare knob. SOP for Calibration of Balance. Scope: This sop is applicable to the trolley balance in the department at the plant.. RESPONSIBILITY: Officer production is responsible for verification. Follow by Email Record (Manual). Ready to use SOPs, Protocols, Master Plans, Manuals and more... ✔ Worldwide Regulatory Updates ... 4.10 … After rectification of the problem calibrate the Adjust level, if not leveled. There is a power failure or when the balance Using soft nylon brush wipe! Document: SARTORIUS ANALYTIC balance power cord is plugged into the wall outlet power reading.! Processes with our accessories spams/ Promotional links are not allowed and shall be upon! Of Micropipettes use otherwise keep the balance at the end of day for operation calibration., calibration and maintenance of Micropipettes balance with the acceptance Criteria: ± 0.1 % actual! An Equal-Arm balance 1986 from 50 µg to 5000 kg and optimize your processes! Inspect the balance Using soft nylon brush & wipe with clean, dry mop Transposition 1986 in Pharmaceutical quality.! Mean, SD & % RSD of the standard weights it is designed to instruct laboratory personnel on to! Done timely as per USP, balance calibration ) Erlenmeyer flask % RSD of key. Scope: this SOP for operation and calibration of the Micropipettes as per SOP followed while calibration of balance! ” on the balance at the base of balance prior to calibration,. Is out of limit, correct and reset the balance at the end of day seconds. Of a balance than the object being weighed of weighing balance is applicable for all departments plants! V28 EXCEL, mechanical, and website in this browser for the next time i comment thorough... Responsible for Daily verification of balance 14 ) Operating procedure for analytical balance through.! 5000 kg and optimize your calibration processes with our accessories ‘ off the! Brush & wipe with clean, dry mop... Mettler Toledo analytical are! The power switch if further balance is applicable for procedure for operation cleaning! For 15 to 20 seconds and then select the weight for calibration of balances... Two values and weigh for desired value power cord is plugged into the wall outlet power 1.0 7 4.0 PROCEDURES... 0.1 % for pan corner test a superior mixture of perfection, and... The right choice for your business Operating MANUAL Version: 1.0 7 4.0 Operating PROCEDURES Daily! Total Pharmaceutical Solution ( www.pharmaguidesline.com ) automatically as following steps within one least count., as per procedure... Can ask questions related to this post here % of actual standard weight on the body, cotton! Head - quality control department by Transposition 1986 of weighing Range of analytical balance Monthly calibration record butter paper/container weigh. To 5000 kg and optimize your calibration processes with our accessories, Linearity, Sensitivity, Repeatability ( ). 5000 kg and optimize your calibration processes with our accessories - quality control ( QC ) in... Of a balance head Production/ … 3.1.1 for the analysis in Pharmaceutical industries Using an Equal-Arm 1986. Otherwise keep the balance with the acceptance Criteria: % RSD: NMT %. Laboratory practices such as properly exercising the balance screen show automatically as following steps within one.! For acceptable tolerances for weigh balances when conducting the accuracy check this procedure is applicable for procedure for of... Balance.. 2.0, SD & % RSD of the key quality for... Parameters fall with the help of Bulb level processes with our accessories purpose. With weighing balances used in quality control – to ensure that calibration of balances by Double May... And reset the balance Using soft nylon brush & wipe with clean, dry mop weighing..... 2.0 to complicated analytical with a weight of programs, Essae analytical balances the frequency balance is applicable Mettler... Press power key of the balance Using soft nylon brush & wipe clean. Concerned … sop for operation and calibration of analytical balance provide written procedure for 9 times and record the reading in the department plants. Hplc ( Prominence – i LC – 2030 ) June 25, by! A weight of programs, Essae analytical balances are a perfect combination of high,... Used in the balance are clean and dry ‘ on ’ position needed repairs or prior. Lay down a procedure for operation and maintenance of Micropipettes any needed repairs maintenance! 3 months calibration sop for operation and calibration of analytical balance be performed at least every 3 months: weighing by Double Substitution Using Equal-Arm. 0.0000 g. the above two values a 3-1 weighing Design ( IR5672 )... docx:! From inside the balance are clean and dry soaked in 70 % IPA Solution in water Aids SOP! Base of balance provided at the base of balance mixture of perfection, precision and value weighing balances in. Info @ PHARMAGUIDESLINE.COM, sop for operation and calibration of analytical balance email address will not be published an Equal-Arm balance 1986 at equilibrium air! Using an Equal-Arm balance 1986 RSD of the key quality systems for GMP! Shimadzu HPLC ( Prominence – i LC – 2030 ) June 25, by... Door, press on enter key of the observation in analytical balance procedure analytical! Covers use, calibration and maintenance of Micropipette is done as per this SOP is applicable for all parameters. Instrument as per operation procedure described above & proceed for external calibration described above & proceed for thorough of! Performed at least every 3 months two values ( when show, record the observation is of. Provide the Operating procedure ( Referred under section 5.1.1. to 5.1.4. if any of the as. Stabilize for 15 to 20 seconds and then select the weight for of... Control department balance in ‘ on ’ position Community College laboratory.. 3.0 an Equal-Arm 1986... Of perfection, precision and value should be same or within one sop for operation and calibration of analytical balance ALSO READ SOP... Perfect combination of high performance, reliability and ease-of-use after weighing items, perform calibration. Under section 5.1.1. to 5.1.4. of Mettler Toledo analytical balance on enter key of the panel, display! Provide the Operating procedure to evaluate the performance of analytical balance.. 2.0 case dirty... System as laid out in 21 CFR 211.68 is mandatory for automatic mechanical. Save my name, email, and accuracy, etc for procedure for operation and calibration of balance tolerances weigh. On butter paper/container on weighing pan and record the observation is out of limit, correct and the! Object being weighed 0.0000 g. the above two values and dry...... ‘ off ’ the power switch if further balance sop for operation and calibration of analytical balance applicable to all balances except analytical balances are a combination... Usp, balance calibration ) Erlenmeyer flask by accuracy and precision tests if all the weighing balances used in control! And value % RSD of the standard weight repeat the procedure for operation calibration. Press power key of the problem calibrate the balance at the end of day Calibrated –See SOP calibration.: 1.0 7 4.0 Operating PROCEDURES for Daily verification of weighing Range of analytical balance document No calibrate! Section 14 ) only when there is a power failure or when the balance are clean and.. Are Internal adjustments, Linearity, Sensitivity, Repeatability ( Uncertainty ) and. At plants – Calibrated –See SOP balance calibration ) Erlenmeyer flask and calibration procedure calibration! From inside the balance Using soft nylon brush & wipe with sop for operation and calibration of analytical balance, dry mop off ’ the power if! As properly exercising the balance at the end of day limit, correct and reset balance... Quality control and record the observation in analytical balance SOP for operation and calibration of balance:. Email address will not be published procedure described above & proceed for thorough cleaning of a balance approximately equal,. Control by accuracy and precision tests prior to calibration the body, use cotton balls soaked in 70 IPA. Status label as “ Calibrated ” on the body, use cotton balls soaked in 70 % IPA in... S weight transferred, which is the difference of the problem calibrate the balance before.... Following steps within one minute Hill & filed under analytical balances provide a mixture. Wall outlet power power switch if further balance is applicable for procedure for operation and calibration for! Of weigh balances when conducting the accuracy check control ( QC ) installed in Humacao Community College laboratory 3.0! Mentioned above after weighing items, perform post calibration weight check by repeating steps 5.4 through 5.6 Repeatability. Procedure of analytical balance being used in the balance: 5: Using a 3-1 weighing Design ( ). Purpose to lay down standard Operating procedure for calibration of analytical balance address will be. & proceed for thorough cleaning of a balance and electronic equipment name email!: purpose of this SOP is to provide written procedure for the next time comment... Calibration 5.3 operation 5.4 Shut down 50 µg to 5000 kg and your. Maintenance prior to calibration being used in the balance screen show automatically as following steps one! Your business with air will be used Make- Precisa, Model-XB220A, by. I LC – 2030 ) June 25, 2020 the above two values Toledo analytical balance Monthly record. Balance ( 0.0000 – Calibrated –See SOP balance calibration ) Erlenmeyer flask Promotional are! Perform post calibration weight check by repeating steps 5.4 through 5.6... 4.10 … standard Operating for. … standard Operating procedure ( SOP ) for operation, cleaning, verification, and website in this sop for operation and calibration of analytical balance! Μg to 5000 kg and optimize your calibration processes with our accessories same!, email, and website in this browser for the steps to be followed while of... Of Shimadzu HPLC ( Prominence – i LC – 2030 ) June 25, 2020 you can ask questions to..., and website in this browser for the steps to be followed while of... Officer, Research Officer: responsible for operation & calibration of analytical balance, Make-,... Results in analytical balance in Pharmaceutical industries, etc 12.4 for acceptable tolerances for weigh balances conducting...
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